Bromine in PDB 242d: Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution.

The structure of Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution., PDB code: 242d was solved by M.R.Peterson, S.J.Harrop, S.M.Mcsweeney, G.A.Leonard, A.W.Thompson, W.N.Hunter, J.R.Helliwell, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	8.00 / 1.65
Space group	P 21 21 21
Cell size a, b, c (Å), α, β, γ (°)	17.970, 30.980, 44.850, 90.00, 90.00, 90.00
R / Rfree (%)	n/a / n/a

The binding sites of Bromine atom in the Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution. (pdb code 242d). This binding sites where shown within 5.0 Angstroms radius around Bromine atom.
In total 2 binding sites of Bromine where determined in the Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution., PDB code: 242d:
Jump to Bromine binding site number: 1; 2;

Bromine binding site 1 out of 2 in the Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution.


Mono view


Stereo pair view

A full contact list of Bromine with other atoms in the Br binding site number 1 of Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution. within 5.0Å range: probe atom residue distance (Å) B Occ A:Br5 b:13.2 occ:1.00 BR A:CBR5 0.0 13.2 1.0 C5 A:CBR5 1.8 6.2 1.0 C4 A:CBR5 2.8 4.7 1.0 C6 A:CBR5 2.8 3.5 1.0 N4 A:CBR5 3.0 5.3 1.0 N4 B:DC7 3.6 6.8 1.0 N9 A:DG4 3.8 3.5 1.0 C2' A:DG4 3.9 4.5 1.0 C8 A:DG4 3.9 9.4 1.0 O A:HOH31 4.0 28.9 1.0 N3 A:CBR5 4.0 4.4 1.0 N1 A:CBR5 4.1 4.1 1.0 C4 A:DG4 4.1 5.5 1.0 O B:HOH67 4.1 28.1 1.0 N7 A:DG4 4.2 5.6 1.0 C1' A:DG4 4.2 4.7 1.0 C4 B:DC7 4.3 4.8 1.0 C5 A:DG4 4.3 4.8 1.0 O6 A:DG6 4.5 7.0 1.0 C2 A:CBR5 4.6 3.5 1.0 N3 A:DG4 4.7 5.0 1.0 C5 B:DC7 4.8 2.3 1.0

Bromine binding site 2 out of 2 in the Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution.


Mono view


Stereo pair view

A full contact list of Bromine with other atoms in the Br binding site number 2 of Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65 A Resolution. within 5.0Å range: probe atom residue distance (Å) B Occ B:Br11 b:14.4 occ:1.00 BR B:CBR11 0.0 14.4 1.0 C5 B:CBR11 1.8 3.3 1.0 C6 B:CBR11 2.8 4.2 1.0 C4 B:CBR11 2.8 2.0 1.0 N4 B:CBR11 3.0 5.4 1.0 N4 A:DC1 3.5 6.8 1.0 C2' B:DG10 3.7 4.7 1.0 N9 B:DG10 3.7 5.7 1.0 C8 B:DG10 3.9 8.7 1.0 C4 B:DG10 4.0 6.3 1.0 N3 B:CBR11 4.0 3.6 1.0 N1 B:CBR11 4.0 2.7 1.0 O B:HOH25 4.0 18.8 1.0 O6 B:DG12 4.1 8.8 1.0 C1' B:DG10 4.1 5.3 1.0 O B:HOH34 4.2 30.5 1.0 C5 B:DG10 4.2 5.6 1.0 N7 B:DG10 4.3 7.8 1.0 C4 A:DC1 4.3 3.4 1.0 O A:HOH21 4.3 19.3 1.0 N3 B:DG10 4.5 4.4 1.0 C2 B:CBR11 4.6 4.5 1.0 C5 A:DC1 4.9 10.7 1.0 C6 B:DG12 4.9 5.4 1.0 N3 A:DC1 5.0 3.9 1.0 C3' B:DG10 5.0 2.0 1.0

M.R.Peterson, S.J.Harrop, S.M.Mcsweeney, G.A.Leonard, A.W.Thompson, W.N.Hunter, J.R.Helliwell. Mad Phasing Strategies Explored with A Brominated Oligonucleotide Crystal at 1.65A Resolution. J.Synchrotron Radiat. V. 3 24 1996.
ISSN: ISSN 0909-0495
PubMed: 16702655
DOI: 10.1107/S0909049595013288